ISOLATION OF CELLULOSE FROM SIWALAN FIBER (BORASSUS FLABELLIFER L.) USING RESPONSE SURFACE METHODOLOGY

YUSUF IKROM NUR AZAMI; IDA MUSFIROH; MUCHTARIDI; RIMADANI PRATIW; OKTA NAMA PUTRA

doi:10.22159/ijap.2023.v15s2.09

Authors

YUSUF IKROM NUR AZAMI Department of Pharmaceutical Analysis and Medicinal Chemistry, Faculty of Pharmacy, Universitas Padjadjaran, West Java, Indonesia
IDA MUSFIROH Department of Pharmaceutical Analysis and Medicinal Chemistry, Faculty of Pharmacy, Universitas Padjadjaran, West Java, Indonesia
MUCHTARIDI Department of Pharmaceutical Analysis and Medicinal Chemistry, Faculty of Pharmacy, Universitas Padjadjaran, West Java, Indonesia
RIMADANI PRATIW Department of Pharmaceutical Analysis and Medicinal Chemistry, Faculty of Pharmacy, Universitas Padjadjaran, West Java, Indonesia
OKTA NAMA PUTRA Department of Pharmaceutical Analysis and Medicinal Chemistry, Faculty of Pharmacy, Universitas Padjadjaran, West Java, Indonesia. Research Center for Agroindustry, National Research and Innovation Agency Soekarno Science and Technology Area, Jakarta-Bogor Street Km. 46, Cibinong, Bogor, 16911, Indonesia

DOI:

https://doi.org/10.22159/ijap.2023.v15s2.09

Keywords:

α-cellulose, Siwalan fiber, Response surface methodology

Abstract

Objective: This study investigated the isolation of α-cellulose powder from siwalan fibers (Borassus flabellifer L.).

Methods: The methods include delignification using 10% NaOH, and bleaching using 10% NaOCl. The present research used response surface methodology (RSM) to investigate the impact of temperature and duration on the bleaching process. Two factors were evaluated and optimized using the central composite design (CCD).

Results: The findings revealed that the hit quality and white degree were 91.5% and 52.58% when the temperature and time of bleaching were 40 °C and 30 min, respectively. Utilizing an analysis of variance (ANOVA), the most influential factors on the percentage of strike quality and whiteness degree were identified. Absorption at 3323.34 cm^-1 for O-H, 2893.22 cm^-1 for C-H, 1371.38 cm^-1 for C-O-H, and 1157.28 cm^-1 for C-O, according to FTIR characterization results, are characteristic cellulose peaks.

Conclusion: The cellulose characterization results acquired in this work show that the temperature in the bleaching process has a significant effect on the cellulose isolation results.

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